Resource Library · SOP 21
Lpg Prover Calibration
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Page 1
SOP 21 – 2019 Page 1 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 SOP 21 Standard Operating Procedure for Calibration of LPG Provers 1 1 Introduction Purpose This...
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SOP 21 – 2019 Page 2 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 All calibration values must have demonstrated metrological traceability to the International Syst...
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SOP 21 – 2019 Page 3 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 All data and appropriate environmental conditions must be documented regardless of calibration lo...
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SOP 21 – 2019 Page 4 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 A calibrated standard prover having a minimum volume of 5 gal is acceptable for 20 gal and 25 gal...
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SOP 21 – 2019 Page 5 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 systematic errors in the prover pressure gauge will be present in field application and use, thus...
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SOP 21 – 2019 Page 6 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 isolation valve will result in errors during the pressurized portion of the prover calibration. T...
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SOP 21 – 2019 Page 7 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 level in the standard from nominal) and water temperature reading in the standard . If multiple t...
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SOP 21 – 2019 Page 8 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 2.4.4.10 Calculate the effective volume of water delivered into the prover using Eqn. 3 or Eqn. 4...
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SOP 21 – 2019 Page 9 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 pressure deformation; all resulting in a drifting pressure setting as the system comes to equilib...
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SOP 21 – 2019 Page 10 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 2.4.6.1 With the pressure in the prover at 100 psig, the prover volume, calculated using the app...
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SOP 21 – 2019 Page 11 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 Final Operations 2.4.7.1 Seal the bottom and top scales as specified by laboratory policy and as...
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SOP 21 – 2019 Page 12 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 These equations correct the volume of water in the unknown prover for the effects of temperature...
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SOP 21 – 2019 Page 13 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 where the water compressibility factor at 60 °F and 100 psig is 1.000322. Caution: Be certain to...
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SOP 21 – 2019 Page 14 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 Calculate the within process standard deviation, s w, for the replicate runs. For two runs, the...
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SOP 21 – 2019 Page 15 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 A standard deviation chart is used for measurement assurance through the evaluation of replicate...
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SOP 21 – 2019 Page 16 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 The standard deviation of the measurement process s p, is taken from a standard deviation chart...
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SOP 21 – 2019 Page 17 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 Table 6. Example uncertainty budget table. Uncertainty Component Description Symbol Source Typic...
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SOP 21 – 2019 Page 18 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 The certificate should also include temperature and pressure correction table s or chart, along...
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SOP 21 – 2019 Page 19 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 Figure 1. Representative LPG Prover Schematic
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SOP 21 – 2019 Page 20 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 Appendix A: Data Recording Sheet LPG Prover Calibration Page 1 of 2 Laboratory Information Metro...
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SOP 21 – 2019 Page 21 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 Appendix A: Data Recording Sheet LPG Prover Calibration Page 2 of 2 Run 2: Data for volumes deli...
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SOP 21 – 2019 Page 22 of 22 This publication is available free of charge from: https://doi.org/10.6028/NIST.IR. 7383 - 2019 Appendix B Example Temperature Correction Table A Example for a 100 gallon prover and 60 °F refe...
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