Resource Library · SOP 28
Advanced Weighing Designs
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Page 1
SOP 28 – 2019 Page 1 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 SOP No. 28 Recommended Standard Operating Procedure for Using Advanced Weighing Designs 1 Introd...
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Page 2
SOP 28 – 2019 Page 2 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 laboratory measurement assurance program to ensure traceability of laboratory standards. Verify...
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Page 3
SOP 28 – 2019 Page 3 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 2 Methodology Scope, Precision, Accuracy This method can be performed on any type of balance or...
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SOP 28 – 2019 Page 4 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 2.3.1. Calibrated reference standards (usually starting at 1 kg or 100 g), calibrated check stan...
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SOP 28 – 2019 Page 5 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 amounts of weight material. Weights should be handled and stored in such a way that they stay cl...
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Page 6
SOP 28 – 2019 Page 6 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 Table 2. Common weighing designs. Design ID Description n Observations d.f. Degrees of freedom R...
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Page 7
SOP 28 – 2019 Page 7 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 and R. C. Raybold, July 1980, with updates to conform to the international formula for calculati...
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Page 8
SOP 28 – 2019 Page 8 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 4.2.Weighing designs integrate a suitable check standard (See GLP 1, SOP 9 and SOP 30). 4.3.The...
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Page 9
SOP 28 – 2019 Page 9 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 Multiple starting restraint schemes with standards calibrated at the same time against the same...
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Page 10
SOP 28 – 2019 Page 10 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 5672 for many additional weighing designs, and variations on the designs noted in this section....
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SOP 28 – 2019 Page 11 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 Using a 5-1 design with two restraints, and the check standard is the difference between the tw...
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Page 12
SOP 28 – 2019 Page 12 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 If a C.1 descending series is used, the following equation is used to calculate the between-tim...
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Page 13
SOP 28 – 2019 Page 13 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 provided in SOP 29 and may be included if corrective action is not taken. ( See NISTIR 6969, SO...
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Page 14
SOP 28 – 2019 Page 14 of 14 This publication is available free of charge from: https://doi. org/10.6028/NIST.IR.5672 - 201 9 factors are considered as a part of the measurement process when obtaining the standard deviati...
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