Resource Library · SOP 7
Single Substitution
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Page 1
SOP 7 – 2019 Page 1 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 SOP 7 Recommended Standard Operating Procedure for Weighing by Single Substitution Using a Single...
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Page 2
SOP 7 – 2019 Page 2 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 Verify that the operator is experienced in precision weighing techniques and has had specific tra...
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Page 3
SOP 7 – 2019 Page 3 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 When steps specific to a particular balance are required, they are given in subsections of the pr...
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Page 4
SOP 7 – 2019 Page 4 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 Symbols Table 2. Symbols used in this procedure. Symbol Description S standard weight X weight ca...
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Page 5
SOP 7 – 2019 Page 5 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 Table 3. Cleaning stabilization. Weight class F1 F2 to M3 After cleaning with alcohol 1 to 2 days...
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Page 6
SOP 7 – 2019 Page 6 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 2.5.1.5 Conduct preliminary measurements to obtain an approximate value for the difference betwee...
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Page 7
SOP 7 – 2019 Page 7 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 2.5.1.7 Adjust the single pan balance or the combination balance so the first two readings of the...
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Page 8
SOP 7 – 2019 Page 8 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 Table 6. Optional Sequence B. Measurement No. Weights on Pan Observation 1 X + tx O1 2 S + ts O2...
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Page 9
SOP 7 – 2019 Page 9 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 3.2.2.1 Optional Sequence A (SXX) ( ) 21 32 1 1 1 1 ( ) 1 sX SX a sw swaa a St t St t X a X M M M...
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Page 10
SOP 7 – 2019 Page 10 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 If requested, the apparent mass versus the reference density of brass may be calculated. This va...
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Page 11
SOP 7 – 2019 Page 11 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 Where SOP 9 is followed, and check standards are used for 2 to 3 nominal values per balance, mor...
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Page 12
SOP 7 – 2019 Page 12 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 Table 7. Example uncertainty budget table. Uncertainty Component Description Symbol Source Typic...
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Page 13
SOP 7 – 2019 Page 13 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 correction value plus the expanded uncertainty must be less than the applicable tolerance to con...
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Page 14
SOP 7 – 2019 Page 14 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 Appendix A Single Substitution Data Sheet (Optional Sequence A, SXX) Laboratory data and conditi...
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Page 15
SOP 7 – 2019 Page 15 of 15 This publication is available free of charge from: https://doi.org /10.6028/NIST.IR .6969 - 2019 Appendix B Single Substitution Data Sheet (Optional Sequence B, XSS) Laboratory data and conditi...
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